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                <text>The virgin oil extraction from avocado Hass was carried using an Abencor pilot scale plant. High-power ultrasound (1.73 MHz) was applied after mixing. High-frequency ultrasound device consists of two transductors which each deliver 30 W/L. Different proportions of water were added before ultrasound treatment (no water added and paste:water relation (1:3, 1:2, 1:1, 2:1, 3:1) and also different ultrasound application times (0, 1, 2, 3, 4, 5, 10, 15, 20 and 25 minutes). The study was carried out by setting one of the two variables considered and changing the values of the other. In the water addition study, ultrasound time was set at 15 min. It was found that oil recovery increased with the percentage of water added. It was decided to employ a ratio of 1:1 to study the influence of ultrasound application time. Under these conditions, it was found that with 1 minute of ultrasound application, recovery increased by 40 % over the process without ultrasound. It was observed that the composition in fatty acids and the content of natural antioxidants (tocopherols and polyphenols) are not affected by the ultrasound application. It is concluded that the application of high-frequency ultrasound with addition of water post malaxing improves recovery of virgin avocado oil without negative effects on the general quality of the oil.</text>
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&lt;p&gt;(Por favor lea este aviso antes de abrir los documentos u objetos)&lt;/p&gt;&#13;
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&lt;p&gt;(Por favor lea este aviso antes de abrir los documentos u objetos)&lt;/p&gt;&#13;
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                <text>&lt;strong&gt;Formate Analogs as Antagonists of the Sex Pheromone of the Honeydew Moth, Cryptoblabes gnidiella : Electrophysiological, Behavioral and Field Evidence.&lt;/strong&gt;</text>
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                <text>Cryptoblabes gnidiella Milli&amp;eacute;re (Lepidoptera: Pyralidae) is an economically important exotic pest of vineyards in Southern Brazil and Uruguay. The sex pheromone of C. gnidiella was identified as a mixture of (Z)-11-hexadecenal and (Z)-13-octadecenal, and has been used to monitor populations of this pest in Israel. The development of mating disruption for this species may be hampered by the chemical instability of the natural pheromone components. Therefore, studies on more stable pheromone analogs may provide tools for a control strategy based on behavior-modifying chemicals. We report here the electrophysiological and behavioral responses of C. gnidiella males to (Z)-9-tetradecenyl formate and (Z)-11-hexadecenyl formate, structural analogs of the pheromone components. In gas chromatography-electroantennogramdetection (GC-EAD) studies, both analogs elicited responses from C. gnidiella male antennae. Pre-exposure to the formates did not affect the subsequent EAD responses to the natural pheromone components. The formates acted as pheromone antagonists in wind tunnel tests, inhibiting the responses of males toward both synthetic pheromone and calling females. In the field, captures of males in pheromone-baited traps decreased, in a dose-response pattern, when different amount of formates were added to the pheromone. These pheromone antagonists, thus, are potentially useful as mating disruptants for C. gnidiella in commercial vineyards.</text>
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                <text>&lt;strong&gt;Sellanes, Carolina&lt;/strong&gt;</text>
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                <text>Journal of Chemical Ecology v. 36, no. 11, 2010. -- p. 1234-1240</text>
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                <text>&lt;p&gt;&lt;strong&gt;Informaci&amp;oacute;n sobre Derechos de Autor&lt;/strong&gt;&lt;/p&gt;&#13;
&lt;p&gt;(Por favor lea este aviso antes de abrir los documentos u objetos)&lt;/p&gt;&#13;
&lt;p&gt;&lt;strong&gt;La legislaci&amp;oacute;n uruguaya&lt;/strong&gt; protege el derecho de autor sobre toda creaci&amp;oacute;n literaria, cient&amp;iacute;fica o art&amp;iacute;stica, tanto en lo que tiene que ver con sus derechos morales, como en lo referente a los derechos patrimoniales con sujeci&amp;oacute;n a lo establecido por el derecho com&amp;uacute;n y las siguientes leyes&lt;/p&gt;&#13;
&lt;p&gt;(LEY 9.739 DE 17 DE DICIEMBRE DE 1937 SOBRE PROPIEDAD LITERARIA Y ARTISTICA CON LAS MODIFICACIONES INTRODUCIDAS POR LA LEY DE DERECHO DE AUTOR Y DERECHOS CONEXOS No. 17.616 DE 10 DE ENERO DE 2003, LEY 17.805 DE 26 DE AGOSTO DE 2004, LEY 18.046 DE 24 DE OCTUBRE DE 2006 LEY 18.046 DE 24 DE OCTUBRE DE 2006)&lt;/p&gt;&#13;
&lt;p&gt;&lt;strong&gt;ADVERTENCIA&lt;/strong&gt; - La consulta de este documento queda condicionada a la aceptaci&amp;oacute;n de las siguientes condiciones de uso: Este documento es &amp;uacute;nicamente para usos privados enmarcados en actividades de investigaci&amp;oacute;n y docencia. No se autoriza su reproducci&amp;oacute;n con fines de lucro. Esta reserva de derechos afecta tanto los datos del documento como a sus contenidos. En la utilizaci&amp;oacute;n o cita de partes debe indicarse el nombre de la persona autora.&lt;/p&gt;</text>
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                  <text>Versiones electrónicas de las tesis de doctorado, maestría y trabajos de diploma de la Facultad de Química, Universidad de la República (UdelaR).&#13;
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                <text>&lt;strong&gt;S&amp;iacute;ntesis de heterociclos como potenciles agentes antihelm&amp;iacute;nticos y citot&amp;oacute;xicos basados en productos naturales de origen marino&lt;/strong&gt;</text>
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                <text>&lt;p&gt;&lt;em&gt;&lt;strong&gt;Informaci&amp;oacute;n sobre Derechos de Autor&lt;/strong&gt; &lt;/em&gt;&lt;/p&gt;&#13;
&lt;p&gt;(Por favor lea este aviso antes de abrir los documentos u objetos)&lt;/p&gt;&#13;
&lt;p&gt;&lt;em&gt;&lt;strong&gt;La legislaci&amp;oacute;n uruguaya protege&lt;/strong&gt;&lt;/em&gt; el derecho de autor sobre toda creaci&amp;oacute;n literaria, cient&amp;iacute;fica o art&amp;iacute;stica, tanto en lo que tiene que ver con sus derechos morales, como en lo referente a los derechos patrimoniales con sujeci&amp;oacute;n a lo establecido por el derecho com&amp;uacute;n y las siguientes leyes (LEY 9.739 DE 17 DE DICIEMBRE DE 1937 SOBRE PROPIEDAD LITERARIA Y ARTISTICA CON LAS MODIFICACIONES INTRODUCIDAS POR LA LEY DE DERECHO DE AUTOR Y DERECHOS CONEXOS No. 17.616 DE 10 DE ENERO DE 2003, LEY 17.805 DE 26 DE AGOSTO DE 2004, LEY 18.046 DE 24 DE OCTUBRE DE 2006 LEY 18.046 DE 24 DE OCTUBRE DE 2006)&lt;/p&gt;&#13;
&lt;p&gt;&lt;strong&gt; ADVERTENCIA -&lt;/strong&gt; La consulta de este documento queda condicionada a la aceptaci&amp;oacute;n de las siguientes condiciones de uso: Este documento es &amp;uacute;nicamente para usos privados enmarcados en actividades de investigaci&amp;oacute;n y docencia. No se autoriza su reproducci&amp;oacute;n con fines de lucro. Esta reserva de derechos afecta tanto los datos del documento como a sus contenidos. En la utilizaci&amp;oacute;n o cita de partes debe indicarse el nombre de la persona autora.&lt;/p&gt;</text>
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                <text>The results from the synthesis of peptides by Fmoc/SPPS on a 2-CTC resin and then lactamization in solution or solid phase for the preparation of cyclopeptides are presented. Both procedures allow the synthesis of the desired compounds in good to very good yield and with high cyclization efficiency for on-resin macrocyclization. In addition, the activities of the corresponding cyclopeptides against the chloroquine-resistant K1 strain of Plasmodium falciparum were evaluated. Cyclo-Cys(Trt)-Gly-Thr( tBu)-Gly-Cys(Trt)-Gly showed potent in vitro and selective activity against this parasite, EC50 = 28 nM.</text>
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&lt;p&gt;(Por favor lea este aviso antes de abrir los documentos u objetos)&lt;/p&gt;&#13;
&lt;p&gt;&lt;strong&gt;La legislaci&amp;oacute;n uruguaya protege el derecho&lt;/strong&gt; de autor sobre toda creaci&amp;oacute;n literaria, cient&amp;iacute;fica o art&amp;iacute;stica, tanto en lo que tiene que ver con sus derechos morales, como en lo referente a los derechos patrimoniales con sujeci&amp;oacute;n a lo establecido por el derecho com&amp;uacute;n y las siguientes leyes (LEY 9.739 DE 17 DE DICIEMBRE DE 1937 SOBRE PROPIEDAD LITERARIA Y ARTISTICA CON LAS MODIFICACIONES INTRODUCIDAS POR LA LEY DE DERECHO DE AUTOR Y DERECHOS CONEXOS No. 17.616 DE 10 DE ENERO DE 2003, LEY 17.805 DE 26 DE AGOSTO DE 2004, LEY 18.046 DE 24 DE OCTUBRE DE 2006)&lt;/p&gt;&#13;
&lt;p&gt;&lt;strong&gt;ADVERTENCIA -&lt;/strong&gt; La consulta de este documento queda condicionada a la aceptaci&amp;oacute;n de las siguientes condiciones de uso: Este documento es &amp;uacute;nicamente para usos privados enmarcados en actividades de investigaci&amp;oacute;n y docencia. No se autoriza su reproducci&amp;oacute;n con fines de lucro. Esta reserva de derechos afecta tanto los datos del documento como a sus contenidos. En la utilizaci&amp;oacute;n o cita de partes debe indicarse el nombre de la persona autora.&lt;/p&gt;</text>
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                <text>Este informe describe la aplicaci6n de una columna de discos rotatorios a la extracc16n de soluc10nes acuoosaa dilu1das de fUrfural con monoclorobenceno. Dentro del rango de variaci6n de las condiciones opeeratorias ensayado, la efic1encia maxima de extracci6n fUe del 92~. Las concentraciones de equilibr10 determinadas expeerimentalmente se correlacionaron con la ecuaci6n de Othmer, pud1endo as! calcularse la curva de equillbrl0. Del estudio de los voldmenes retenidos surge la exlsstenc1a de dos reg1menes hidrodinamicos. Para el r6gimen de baja velocidad de rotaci6n se hal16 la siguiente correlaci6n: (Vn.JJ /rr) = 7,71 x 10-6 .NO.6t . C Para el otro r~gimen se recomienda hacer ensayos a velocidades de rotac16n mayorea. Tanto los AEET como laa AUT dismlnuyen al aumentar la velocldad de rotaci6n 0 el coclente</text>
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&lt;p&gt;(Por favor lea este aviso antes de abrir los documentos u objetos)&lt;/p&gt;&#13;
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                <text>The preparation and cycloadditions of azidodienes 13 and 14 are described in detail. The synthesis of pyrrolines 1 and 2 is reported, and the conditions are revealed to achieve maximum selectivity in their preparation. The topography of the ultimately prepared pyrrolines depends primarily on the substitution parameters of the starting dienes and on the conditions of rearrangement of their respective vinylaziridines 15 and 16. The former parameter is easily controlled through the vinylogous Reformatsky reaction of ethyl 4-bromocrotonate with aldehyde precursors. The latter parameter depends on the choice of thermolytic vs. nucleophilic activation of particular bonds in vinylaziridines 15 and 16. The flexibility and practicality of this method is exemplified by several convergent approaches to substituted pyrrolines 1 and 2 and their conversion to the title pyrrolizidine alkaloids. Stereospecific preparation of saturated pyrrolizidines 35 is also described. A detailed study of the base-catalyzed elimination of &amp;beta;-acetoxy esters was performed, and the stereochemical consequences are reported for the formation of E and Z geometric isomers of dienes 13.</text>
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                <text>Current Organic Chemistry |g v. 4, , 2000. -- p. 283-304</text>
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                <text>&lt;p&gt;&lt;strong&gt;Informaci&amp;oacute;n sobre Derechos de Autor&lt;/strong&gt;&lt;/p&gt;&#13;
&lt;p&gt;(Por favor lea este aviso antes de abrir los documentos u objetos)&lt;/p&gt;&#13;
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&lt;p&gt;&lt;strong&gt;ADVERTENCIA -&lt;/strong&gt; La consulta de este documento queda condicionada a la aceptaci&amp;oacute;n de las siguientes condiciones de uso: Este documento es &amp;uacute;nicamente para usos privados enmarcados en actividades de investigaci&amp;oacute;n y docencia. No se autoriza su reproducci&amp;oacute;n con fines de lucro. Esta reserva de derechos afecta tanto los datos del documento como a sus contenidos. En la utilizaci&amp;oacute;n o cita de partes debe indicarse el nombre de la persona autora.&lt;/p&gt;</text>
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                <text>Proliferation of macrophages is a hallmark of inflammation in many type 2 settings including helminth infections. The cellular expansion is driven by the type 2 cytokine interleukin-4 (IL-4), as well as by M-CSF, which also controls homeostatic levels of tissue resident macrophages. Cystic echinococcosis, caused by the tissue-dwelling larval stage of the cestode Echinococcus granulosus, is characterised by normally subdued local inflammation. Infiltrating host cells make contact only with the acellular protective coat of the parasite, called laminated layer, particles of which can be ingested by phagocytic cells. Here we report that a particulate preparation from this layer (pLL) strongly inhibits the proliferation of macrophages in response to IL-4 or M-CSF. In addition, pLL also inhibits IL-4-driven up-regulation of Relm-&amp;alpha;, without similarly affecting Chitinase-like 3 (Chil3/Ym1). IL-4-driven cell proliferation and up-regulation of Relm-&amp;alpha; are both known to depend on the phosphatidylinositol (PI3K)/Akt pathway, which is dispensable for induction of Chil3/Ym1. Exposure to pLL in vitro inhibited Akt activation in response to proliferative stimuli, providing a potential mechanism for its activities. Our results suggest that the E. granulosus laminated layer exerts some of its anti-inflammatory properties through inhibition of PI3K/Akt activation and consequent limitation of macrophage proliferation.</text>
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                <text>Scientific Reports v. 6, 2016. -- p. 1-13.-- e39204</text>
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&lt;p&gt;&lt;strong&gt;ADVERTENCIA -&lt;/strong&gt; La consulta de este documento queda condicionada a la aceptaci&amp;oacute;n de las siguientes condiciones de uso: Este documento es &amp;uacute;nicamente para usos privados enmarcados en actividades de investigaci&amp;oacute;n y docencia. No se autoriza su reproducci&amp;oacute;n con fines de lucro. Esta reserva de derechos afecta tanto los datos del documento como a sus contenidos. En la utilizaci&amp;oacute;n o cita de partes debe indicarse el nombre de la persona autora.&lt;/p&gt;</text>
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                <text>&lt;strong&gt;Are consumers willing to pay more for reformulated processed meat products in the context of the implementation of nutritional warnings : Case study with frankfurters in Chile&lt;/strong&gt;</text>
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                <text>The aim of the present work was to assess consumers' willingness to pay for reformulated frankfurters in the context of the implementation of nutritional warnings. Images of frankfurter packages were designed using a fractional factorial design with 5 2-level variables: brand type, sodium reduction, saturated fat reduction, fibre claim and cholesterol claim. An online study with 548 consumers was implemented with Chilean participants, who were asked to indicate how much they would be willing to pay for each of the packages. Data were analysed using analysis of variance and hierarchical cluster analysis. Willingness to pay was significantly affected by brand type and sodium and fat reduction, whereas fibre and cholesterol claim did not have a significant effect. These results suggest that in the context of the implementation of nutritional warnings reformulation of processed meat products should focus on the reduction of key nutrients, although consumers may not be willing to pay a higher price for reformulated products.</text>
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                <text>Meat Science v. 152, 2019. -- p. 104-108</text>
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&lt;p&gt;&lt;strong&gt;ADVERTENCIA -&lt;/strong&gt; La consulta de este documento queda condicionada a la aceptaci&amp;oacute;n de las siguientes condiciones de uso: Este documento es &amp;uacute;nicamente para usos privados enmarcados en actividades de investigaci&amp;oacute;n y docencia. No se autoriza su reproducci&amp;oacute;n con fines de lucro. Esta reserva de derechos afecta tanto los datos del documento como a sus contenidos. En la utilizaci&amp;oacute;n o cita de partes debe indicarse el nombre de la persona autora.&lt;/p&gt;</text>
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                <text>&lt;strong&gt;Endophytic Yeasts for the Biocontrol of Phlyctema vagabunda in Apples&lt;/strong&gt;</text>
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                <text>Bull&amp;rsquo;s-eye rot, produced by Phlyctema vagabunda, is an important postharvest disease in apples. Current measures to control infection include synthetic fungicides, in addition to the&lt;br /&gt;application of copper hydroxide and potassium phosphite. However, growing public concern regarding fungicide residues in food has generated interest in developing non-chemical alternative control methods; biological control is one of the most promising alternatives. In this research, native&lt;br /&gt;endophytic yeasts were isolated and evaluated for the biocontrol of P. vagabunda in apples. The mechanisms of action involved were also determined. Our research found 2 isolates, Vishniacozyma victoriae EPL4.5 and EPL29.5, which exhibited biocontrol activity against P. vagabunda at 20 �C in&lt;br /&gt;apples, the incidence of bull&amp;rsquo;s-eye rot was reduced by 39% and 61%, respectively, and the severity of the disease was decreased by 67% and 70%, respectively, when apples were inoculated with these yeasts 24 h before applying the pathogen. The main mechanisms that could be involved&lt;br /&gt;in the observed biocontrol activity are the ability to form biofilms and the production of volatile organic compounds.</text>
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                <text>Horticulturae v. 8, n&amp;deg;535, 2022. --</text>
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                <text>One hundred twenty-five yeast strains isolated from table grapes and apples were evaluated for the control Botrytis cinerea of in vitro and in vivo. Ten strains were selected for their ability to inhibit mycelial growth of B. cinerea in vitro. In the in vivo assays, these yeasts were tested at 20 ◦C on &amp;lsquo;Thompson Seedless&amp;rsquo; berries for 7 days; only three were selected (m11, me99 and ca80) because they significantly reduced the incidence of gray mold. These three yeast strains were then evaluated at different concentrations (1 &amp;times; 107 , 1 &amp;times; 108 and 1 &amp;times; 109 cells mL&amp;minus;1 ) on &amp;lsquo;Thompson Seedless&amp;rsquo; grape berries at 20 ◦C. The strains m11, me99 and ca80 reduced the incidence of B. cinerea to 11.9, 26.1 and 32.1%, respectively, when the berries were submerged in a yeast suspension at a concentration of 1 &amp;times; 109 cells mL&amp;minus;1 24 h before inoculation with B. cinerea. The most favorable pH for antifungal activity was 4.6 in the three isolates. The three yeast strains secreted the hydrolytic enzymes chitinase and &amp;beta;-1-glucanase, and two strains (me99 and ca80) produced siderophores. The three yeast strains exhibited low oxidative stress tolerance and only strain m11 had the ability to produce biofilms. The strains were identified using 5.8S-ITS rDNA PCR-RFLP and correspond to the Meyerozyma guilliermondii (m11) and Aureobasidium pullulans (me99 and ca80) species.</text>
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                <text>Two catalysts prepared separately by iron pillaring of two different-sized particle fractions of a dried, ground and sieved clay mineral were tested for catalytic performance in photo-Fenton discoloration of methylene blue aqueous solutions. Two different-sized particle fractions of the mineral were selected prior to pillaring, ranging below 250 mm and within the range of 250&amp;ndash; 450 mm, respectively. The resulting solids were characterized by thermogravimetric analysis, nitrogen adsorption isotherms and ultimate analysis at different preparation stages. Significant differences were found in catalyst textural parameters according to the starting mineral particle size, a higher specific surface area, and specific pore volume, was found for the catalyst obtained from the smaller-sized particle fraction of the mineral. Both catalysts showed activity in the discoloration of aqueous dye solution. Differences in catalyst performance were correlated with textural parameters. Trial tests were conducted in different experimental conditions, enabling the assessment of contributions of different catalytic mechanisms</text>
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&lt;p&gt;&lt;strong&gt;La legislaci&amp;oacute;n uruguaya&lt;/strong&gt; protege el derecho de autor sobre toda creaci&amp;oacute;n literaria, cient&amp;iacute;fica o art&amp;iacute;stica, tanto en lo que tiene que ver con sus derechos morales, como en lo referente a los derechos patrimoniales con sujeci&amp;oacute;n a lo establecido por el derecho com&amp;uacute;n y las siguientes leyes&lt;/p&gt;&#13;
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&lt;p&gt;&lt;strong&gt;ADVERTENCIA&lt;/strong&gt; - La consulta de este documento queda condicionada a la aceptaci&amp;oacute;n de las siguientes condiciones de uso: Este documento es &amp;uacute;nicamente para usos privados enmarcados en actividades de investigaci&amp;oacute;n y docencia. No se autoriza su reproducci&amp;oacute;n con fines de lucro. Esta reserva de derechos afecta tanto los datos del documento como a sus contenidos. En la utilizaci&amp;oacute;n o cita de partes debe indicarse el nombre de la persona autora.&lt;/p&gt;</text>
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                <text>A montmorillonite was pillared separately with chromium and aluminum polyoxocations (Cr&amp;ndash;C and Al&amp;ndash;C respectively) and also with an equimolar mixture of both polioxocations (Al&amp;ndash;Cr&amp;ndash;C). The resulting solids were characterized by scanning electron microscopy, energy dispersive spectrometry, thermal analysis, Fourier transform infrared spectroscopy, X-ray diffraction and nitrogen adsorption at �196 �C. The inclusion of polycations in the interlamellar space led to modifications in the properties of the clay. An eleven fold increase in specific surface area with respect to the calcined starting clay was found for the Al&amp;ndash;C, whereas a twofold increase was observed for the Cr&amp;ndash;C; the value for the Al&amp;ndash;Cr&amp;ndash;C was only slightly higher than that for the latter. Diffractograms of the Cr&amp;ndash;C showed the occurrence of a Cr2O3 phase. Catalytic activity in oxidative dehydrogenation of propane was assayed in the temperature range from 350 �C to 450 �C using Ar/C3H8/O2 (80/10/10) as reactant gas mixture. Propylene selectivity was found to be temperature- dependent, showing a maximum in the studied temperature range for the catalyst containing only aluminum, whereas remaining practically constant for the Cr-containing catalysts. Highly promising propylene yields at low temperature were obtained with the catalyst containing Al and Cr (Al&amp;ndash;Cr&amp;ndash;C): 9.3% at 350 �C and 10.3% at 450 �C.</text>
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&lt;p&gt;(Por favor lea este aviso antes de abrir los documentos u objetos)&lt;/p&gt;&#13;
&lt;p&gt;&lt;strong&gt;La legislaci&amp;oacute;n uruguaya&lt;/strong&gt; protege el derecho de autor sobre toda creaci&amp;oacute;n literaria, cient&amp;iacute;fica o art&amp;iacute;stica, tanto en lo que tiene que ver con sus derechos morales, como en lo referente a los derechos patrimoniales con sujeci&amp;oacute;n a lo establecido por el derecho com&amp;uacute;n y las siguientes leyes&lt;/p&gt;&#13;
&lt;p&gt;(LEY 9.739 DE 17 DE DICIEMBRE DE 1937 SOBRE PROPIEDAD LITERARIA Y ARTISTICA CON LAS MODIFICACIONES INTRODUCIDAS POR LA LEY DE DERECHO DE AUTOR Y DERECHOS CONEXOS No. 17.616 DE 10 DE ENERO DE 2003, LEY 17.805 DE 26 DE AGOSTO DE 2004, LEY 18.046 DE 24 DE OCTUBRE DE 2006 LEY 18.046 DE 24 DE OCTUBRE DE 2006)&lt;/p&gt;&#13;
&lt;p style="margin-bottom: 0cm;"&gt;&lt;strong&gt;ADVERTENCIA&lt;/strong&gt; - La consulta de este documento queda condicionada a la aceptaci&amp;oacute;n de las siguientes condiciones de uso: Este documento es &amp;uacute;nicamente para usos privados enmarcados en actividades de investigaci&amp;oacute;n y docencia. No se autoriza su reproducci&amp;oacute;n con fines de lucro. Esta reserva de derechos afecta tanto los datos del documento como a sus contenidos. En la utilizaci&amp;oacute;n o cita de partes debe indicarse el nombre de la persona autora.&lt;/p&gt;&#13;
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                <text>A raw montmorillonite was exchanged with the trinuclear Fe(III) acetate complex and calcined at 400 &amp;deg;C. Ratios of 0.5, 1.0 and 3.5 mmol of complex per gram of clay were employed. The pillared solids (Fe-PILCs) were analyzed by X-ray fluorescence spectroscopy, thermogravimetry analysis, scanning electron microscopy, M&amp;ouml;ssbauer spectroscopy, X-ray diffraction and nitrogen adsorption isotherms. Total iron amount incorporated by the clay increases with the complex/clay ratio used from 6.1% to 17.6%. Iron is incorporated mainly in the interlayer space when the clay is pillared with the smallest complex/clay ratio and a microporous network is generated. Adsorption of iron on the outer surface is favored for higher iron loads and results in the creation of a mesoporous structure. M&amp;ouml;ssbauer analysis shows the presence of iron as maghemite (&amp;gamma;-Fe2O3) particles with a wide particle size distribution. All the Fe-PILCs were active as catalysts for phenol degradation under photo-Fenton like conditions using UVA radiation and a maximum in their activity is achieved for an intermediate iron content (13.4%).</text>
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